1. Clean glassware:
a. Fill glassware to be used with UVTOC water from Millipore
system
dispenser.
b. Sprinkle a little Alconox into vessels with clean water.
c. Ultra-sonic clean in plastic dish so that edges of clean glassware
do
NOT touch edges of ultrasonic cleaner.
d. 15 minutes ultrasonic then pour out Alconox+water and rinse
with
Millipore water.
e. Repeat steps a. - d. two more times.
f. A clean 1 liter beaker can now be filled with Millipore water,
heated, and used as ‘leach’ step for 100 ml beaker. (Leach
100 ml beaker by filling beaker with near-boiling Millipore
water and pour off after 15-30 sec.) Rinse 100 ml beaker with
methanol.
g. Cover cleaned glassware with a loosely-fitting tent of Al
foil
to keep dust from settling onto cleaned surfaces.
2. Use only stainless tweezers (that have been degreased in clean Acetone)
to put wafer into a 100 ml beaker.
3. Fill beaker to half full with Trichloroethlyene.
4. Add enough hot water to small ultrasonic basin (with cold or cooling
water) to make temperature 55 C (NO hotter;since wafers will
shatter if ultrasonically cleaned in hot Acetone due to cavitation
and uncontrolled agitation).
5. Ultrasonically clean at 55 C for 3 minutes with the voltage setting
(on an autotransformer supplying the ultrasonic device) turned
down to 30 V or 40 V AC or so--look for signs of agitation
that should be avoided!
Never measure the temperature of the degreasing solvent directly
with the thermometer since this will simply foul the solution
directly exposed to the wafer.
6. Decant (pour off) solvent into appropriate waste solvent beaker
for appropriate disposal later.
7. Repeat steps 3 through 6 for Acetone then Methanol (3 minutes each
at 55 C).
8. Remove wafer from a small puddle of methanol with stainless tweezers
directly into the stream of dry nitrogen (blow-off from small
dewar
with a 0.22 micron filter in the blow-off line). Dry the wafer
completely, taking care to force the adhered drop of methanol
away from the sensitive area (shiny surface of polished wafer).
A receding, advancing, then receding droplet of methanol will
leave a stain with traces of contamination on the surface of
the
wafer.
The best way to do this operation is to tip the beaker at 45 deg
or so, push the wafer into a position (the edge of the wafer
is off the side and bottom of the beaker) then grasp the
very
edge of the wafer with the tweezer. Practice with a used wafer
before trying this with a properly cleaned wafer.
9. Put wafer into carrier and close lid with dry nitrogen blowing
gently across the wafer carrier.